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Charges
Small Molecule Mass Spectrometry Facility
The schedule lists fees that would
be charged a client from UAMS, CAVHS, BRIN or UALR for non-profit research. Others
will be charged a percentage of the scheduled fees, as follows:
Cancer Center (ACRC) Affiliates, Nonprofit........83%
UAMS, CAVHS, BRIN, and UALR, Nonprofit....100%
External, Nonprofit.................................................115%
Commercial...........................................................165%
| University of Arkansas for Medical Sciences |
|
| Mass Spectrometry of
Multiple Small Molecules Core Facility — Fee Schedule…………… |
A |
| MS/msm |
Setup feea |
Per-Lot process feea,b |
Process Lot (max # units) |
Per-Unit process feea |
Billing Unit |
e.g., Total
Charge for 10 Units |
Per-Lot turnaroundc (bus. days) |
|
| Multiple small molecules
services |
|
|
|
|
|
|
|
|
|
Specimen bank — creation
and storage of homogeneous lyophilizates |
|
|
|
|
|
|
Full banking, solvent-free (SF)
protocol (includes "cryo-cart" service, vials,
stoppers, freeze drying, dry pulverization, dry mass determination, pH
determination, onsite storage, data management and up to 5 aliquot removals) |
|
$40 |
40 |
$1.26 |
frozen specimen |
|
1.5 |
|
|
|
Full banking, lipid extraction
(LX) protocol (Required for assays of oxidative damage, i.e., assays 8-12 below. Same as the prior service, except with
lipid extraction inserted before or after freeze drying. Both lipid and
non-lipid fractions are dried and banked.) |
|
$36 |
24 |
$3.52 |
frozen specimen |
|
2.5 |
|
|
Assays on homogeneous
lyophilizate samples (greyed-out assays are in
development, with target dates indicated) |
|
1a |
Thiols & disulfides panel #1 (free, oxidized and reduced) |
|
$250 |
24 |
$7 |
sample |
|
2 |
1/15/04 |
|
1b |
Thiols & disulfides (total, borohydride-reduced, requires 1a prep) |
|
$75 |
24 |
$6 |
sample |
|
2 |
1/15/04 |
|
2 |
Energy charge
(adeninosine phosphate ratios: AMP, ADP &
ATP) |
|
|
24 |
|
sample |
|
|
2/1/04 |
|
3 |
Nicotine and flavin adenine
dinucleotides |
|
|
24 |
|
sample |
|
|
2/15/04 |
|
4 |
Gluconeogenic & Krebs Cycle
flux |
|
|
|
|
sample |
|
|
6/1/04 |
|
5 |
Amino acid panel |
|
|
|
|
sample |
|
|
8/1/04 |
|
6 |
Metabolic fingerprinting |
|
|
|
|
sample |
|
|
3/1/04 |
|
7 |
Metabolomics |
|
|
|
|
sample |
|
|
6/1/04 |
|
8 |
4-Hydroxynonenal |
|
|
|
|
sample |
|
|
4/1/04 |
|
9a |
F2α-Isoprostanes, free |
|
$200 |
12 |
$65 |
sample |
|
2 |
12/10/03 |
|
9b |
F2α-Isoprostanes, bound |
|
$395 |
12 |
$115 |
sample |
|
2 |
1/1/04 |
|
10a |
F4-Neuroprostanes, free |
|
|
20 |
|
sample |
|
|
3/1/04 |
|
10b |
F4-Neuroprostanes, bound |
|
|
20 |
|
sample |
|
|
3/1/04 |
|
11a |
DNA adducts panel I (8-0xoguanine, other modified bases released by fpg enzyme.) |
|
$208 |
16 |
$8.39 |
sample |
|
2 |
1/1/04 |
|
11b |
DNA adducts panel II (5-methyl-2'-deoxycytidine, other modified nucleotides
released by exhaustive nuclease digestion) |
|
|
16 |
|
sample |
|
|
1/1/04 |
|
12 |
Protein 3-nitrotyrosine |
|
|
20 |
|
sample |
|
|
5/1/04 |
| University of Arkansas for Medical
Sciences |
|
| Small Molecule Mass Spectrometry Facility — Fee Schedule
A |
|
|
|
|
Setup feea |
Per-Lot process feea,b |
Lot Size (max # units) |
Per-Unit process feea |
Unit |
e.g., cost for
10 Units |
Turn- aroundc (bus.days) |
|
| Basic services, a la carte |
|
|
|
|
|
|
|
|
|
Mass spectrometry (small molecules) |
|
|
|
|
|
|
|
|
|
Mass determination (MS scan) |
|
|
|
$22 |
compound |
$220 |
1 |
|
|
MS/MS
(Product-ion, precursor-ion or constant-neutral-loss scan) |
|
|
|
$36 |
compound |
$360 |
1 |
|
|
|
LC-MS
(includes LC-MS/MS) |
|
|
|
$36 |
hour |
$360 |
-- |
|
|
High performance liquid
chromatography |
|
|
|
|
|
|
|
|
LC-UV |
|
|
|
$24 |
hour |
$240 |
-- |
|
|
LC-EC |
|
|
|
$29 |
hour |
$290 |
-- |
|
|
LC-MS
(includes LC-MS/MS) |
|
|
|
$36 |
hour |
$360 |
-- |
|
|
LC with >1 detector (LC-UV/MS, LC-UV/EC, LC-EC/MS, LC-UV/EC/MS) |
|
|
|
$42 |
hour |
$420 |
-- |
|
|
Validated Assays (future assays not shown) |
|
|
|
|
|
|
|
|
1a |
Thiols & disulfides panel #1 (free, oxidized and reduced) |
|
$250 |
24 |
$7 |
specimen |
$320 |
2 |
1/5/04 |
|
1b |
Thiols & disulfides (total, borohydride-reduced) |
|
$75 |
24 |
$6 |
specimen |
$135 |
2 |
1/5/04 |
|
2 |
Energy charge
(adeninosine phosphate ratios: AMP, ADP &
ATP) |
|
24 |
|
specimen |
|
|
1/22/04 |
|
3 |
Nicotine and flavin adenine
dinucleotides |
|
24 |
|
specimen |
|
|
2/5/04 |
|
4 |
Gluconeogenic & Krebs Cycle
flux |
|
|
|
specimen |
|
|
5/22/04 |
|
5 |
Amino acid panel |
|
|
|
specimen |
|
|
7/22/04 |
|
6 |
Metabolic fingerprinting |
|
|
|
specimen |
|
|
2/20/04 |
|
7 |
Metabolomics |
|
|
|
specimen |
|
|
5/22/04 |
|
8 |
4-Hydroxynonenal |
|
|
|
specimen |
|
|
3/22/04 |
|
9a |
F2α-Isoprostanes, free |
|
$200 |
12 |
$65 |
specimen |
$850 |
2 |
|
|
9b |
F2α-Isoprostanes, bound |
|
$395 |
12 |
$115 |
specimen |
$1,545 |
2 |
|
|
10a |
F4-Neuroprostanes, free |
|
20 |
|
specimen |
|
|
2/20/04 |
|
10b |
F4-Neuroprostanes, bound |
|
20 |
|
specimen |
|
|
2/20/04 |
|
11a |
DNA adducts panel I (8-0xoguanine, other modified bases released by fpg enzyme) |
|
$208 |
16 |
$8 |
specimen |
|
2 |
12/22/03 |
|
11b |
DNA adducts panel II (5-methyl-2'-deoxycytidine, other modified nucleotides
released by exhaustive nuclease digestion) |
|
16 |
|
specimen |
|
|
12/22/03 |
|
12 |
Protein 3-nitrotyrosine |
|
20 |
|
specimen |
|
|
4/21/04 |
|
Specimen handling |
|
|
|
|
|
|
|
|
|
|
Cryo-cart service |
|
$6.50 |
40 |
$0.55 |
specimen |
$12 |
-- |
|
|
|
Freeze-drying |
|
$15 |
80 |
$0.35 |
specimen |
$19 |
1.5 |
|
|
|
Lipid extraction |
$2.00 |
$48 |
24 |
$1.00 |
specimen |
$60 |
1 |
|
|
|
Pulverization |
$2.00 |
|
|
$2.00 |
specimen |
$22 |
1 |
|
|
|
Mass & pH determination |
|
|
|
$0.60 |
specimen |
$6 |
0.2 |
|
|
|
Storage and Data Management (freeze-dried samples only) |
|
|
|
$1.80 |
specimen |
$18 |
0.1 |
|
|
|
Aliquot removal |
$3.00 |
|
|
$0.60 |
aliquot |
$9 |
0.2 |
|
|
|
Full banking, solvent-free (SF)
protocol (includes "cryo-cart" service, vials,
stoppers, freeze drying, dry pulverization, dry mass determination, pH
determination, onsite storage, data management and up to 5 aliquot removals) |
|
$40 |
40 |
$1.26 |
frozen specimen |
$53 |
1.5 |
|
|
|
Full banking, lipid extraction
(LX) protocol (Required for assays of oxidative damage, i.e., assays 8-12 below. Same as the prior service, except with
lipid extraction inserted before or after freeze drying. Both lipid and
non-lipid fractions are dried and banked.) |
|
$36 |
24 |
$3.52 |
frozen specimen |
$71 |
2.5 |
|
|
 |
